TECHNICAL ANALYSIS LAB 6TH SEMESTER DIPLOMA IN CHEMICAL ENGINEERING

 

BOARD OF TECHNICAL EDUCATION

DIPLOMA IN CHEMICAL ENGINEERING

CLASS                       :           VI SEMESTER

SUBJECT                  :           TECHNICAL ANALYSIS LAB

SUBJECT CODE     :           9CH66P

                                                                                                No of Hrs/week: 06 Hrs

                                                                                                Total No. of. Hrs: 96 Hrs

SYLLABUS

LIST OF EXPERIMENTS :

1.    Determine the acidity of water.

2.    Determine the chloride content of water

3.    Determine the total dissolved solids in water.

4.    Determine the BOD & COD of water.

5.    Determine the percentage ammonia content of the given homogenous fertilizer (ammonium sulphate ) volumetrically , using NaOH and standard  acid.

6.    Determine the moisture content in grease.

7.    Determine the moisture content in the given soap sample 

8.    Determine the % of fatty matters content in soap sample by wax cake method.

9.    Determine the calcium carbonate in the given sample of limestone.

10.  Glycerol estimation by Di-chromate method.

11.  Determine the saponification value of oil.

12.  Determine the Iodine value of given sample of oil.

13.  Determine the acid value of the given oil sample.

14.  Determine the flash and fire point of given sample of oil.

15.  Determine the specific gravity of given sample oil.

16.  Determine the viscosity of the given sample of oil using Ostwald viscometers.

17.  Determine the viscosity of the given sample of oil using red-wood viscometers.

18.  Analysis of cement to determine the total % of calcium oxide and magnesium oxide.

19.  Calorific value by Bomb calorimeter.

20.  Proximate anlysis of coal

a)      Moisture content.

b)      Volatile matter.

c)      Ash content.

 

SCHEME of EVALUATION:

 

Sl.No.

Scheme

Marks Allotted

1

Record

05

2

Procedure

15

3

Conducting

25

4

Calculation

30

5

Result

05

6

Viva

20

 

TOTAL

100

 

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